DES-based vortex-assisted liquid-liquid microextraction procedure developed for the determination of paraben preservatives in mouthwashes

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dc.contributor.authorDalmaz, Aslıhan
dc.contributor.authorOzak, Sezen Sivrikaya
dc.date.accessioned2023-07-26T11:58:43Z
dc.date.available2023-07-26T11:58:43Z
dc.date.issued2022
dc.departmentDÜ, Sağlık Bilimleri Enstitüsü, Doğal, Bitkisel Ürünler ve Kozmetik Ürünler Ana Bilim Dalıen_US
dc.description.abstractA green deep eutectic solvent-based vortex-assisted liquid-liquid microextraction (DES-VALLME) procedure for the determination of parabens in mouthwashes was developed. Deep eutectic solvents formed by combining DLmenthol and decanoic acid in different mol ratios were prepared, the highest extraction recovery was obtained with DES consisting of 4:1 M ratio, and this DES was used as an extraction solvent for paraben determination in mouthwashes. The effect of parameters such as solution pH, mol ratio of DES composition, DES volume, vortex and centrifugation time and sample volume were examined. Optimum working conditions of the study; 400 mu L DES, 3 min. vortex time, 5 min. centrifugation time, 5 mL sample volume were determined. The detection limit was in the range of 4.6-6.1 mu g L-1, while the RSDs values were in the range of 0.70-1.41% in intraday and 1.27-2.41% in interday. The method in the study was successfully applied for the determination of methyl, ethyl, propyl and butyl paraben in 10 different mouthwashes obtained from cosmetic stores..en_US
dc.description.sponsorshipDuzce University Scientific Research Projects Fund [2021-05-03-1252]; Turkey's Council of Higher Education (CoHE) 100/2000 doctoral scholarship program; CoHEen_US
dc.description.sponsorshipThis research was supported by Duzce University Scientific Research Projects Fund (Project No: 2021-05-03-1252) and Turkey's Council of Higher Education (CoHE) 100/2000 doctoral scholarship program. The authors would like to thank the Duzce University Scientific Research Projects Fund and CoHE for contributing to the financial portion of the project.en_US
dc.identifier.doi10.1016/j.microc.2022.107445
dc.identifier.issn0026-265X
dc.identifier.issn1095-9149
dc.identifier.scopus2-s2.0-85127726076en_US
dc.identifier.scopusqualityQ1en_US
dc.identifier.urihttps://doi.org/10.1016/j.microc.2022.107445
dc.identifier.urihttps://hdl.handle.net/20.500.12684/13553
dc.identifier.volume179en_US
dc.identifier.wosWOS:000793744500003en_US
dc.identifier.wosqualityQ1en_US
dc.indekslendigikaynakWeb of Scienceen_US
dc.indekslendigikaynakScopusen_US
dc.institutionauthorDalmaz, Aslıhan
dc.institutionauthorSivrikaya Özak, Sezen
dc.language.isoenen_US
dc.publisherElsevieren_US
dc.relation.ispartofMicrochemical Journalen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.snmz$2023V1Guncelleme$en_US
dc.subjectParabens; Green Chemistry; Microextraction; Deep Eutectic Solvent; Preservatives; Mouthwashen_US
dc.subjectDeep Eutectic Solvent; Solid-Phase Microextraction; Personal Care Products; Gas-Chromatography; Extraction; Preconcentration; Absorption; Dispersion; Separation; Beveragesen_US
dc.titleDES-based vortex-assisted liquid-liquid microextraction procedure developed for the determination of paraben preservatives in mouthwashesen_US
dc.typeArticleen_US

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