Green synthesis of environmentally friendly Ag/AgCl nanoparticles for use as solid phase extraction materials
Küçük Resim Yok
Tarih
2025
Dergi Başlığı
Dergi ISSN
Cilt Başlığı
Yayıncı
Taylor & Francis Inc
Erişim Hakkı
info:eu-repo/semantics/closedAccess
Özet
Green synthesis is a prominent procedure used to easily and environmentally friendly fabricate nanostructures and nanoparticles (NPs), without complex instrumentation, intricate procedures, and harmful chemicals. This study investigated the green synthesis of silver NPs (AgNPs), with Aronia melanocarpa fruit extract as the reducing agent. Following synthesis optimization, AgNPs were characterized using a range of analytical techniques, including UV-Vis, XRD, SEM-EDX, BET, and TEM analyses. Based on the characterization results, an Ag/AgCl hybrid structure was formed. The Ag/AgCl NPs obtained were utilized as adsorbents to remove Cd(II) and Pb(II) heavy metals. The experimental factors that were optimized included pH (5.5), sample volume (5 mL), eluent type and concentration (2 M HNO3), adsorbent amount (5 mg), and extraction time (30 min). Under optimized conditions, the limits of detection were determined to be 9.6 and 4.8 mu g/L for Pb(II) and Cd(II), respectively. These limits were established within a concentration range of 50-3,000 mu g/L.
Açıklama
Anahtar Kelimeler
[Keyword Not Available]
Kaynak
Journal of Environmental Science and Health Part A-Toxic/Hazardous Substances & Environmental Engineering
WoS Q Değeri
Q3
Scopus Q Değeri
Q2
Cilt
60
Sayı
13
