Development of clinoptilolite zeolite-coated magnetic nanocomposite-based solid phase microextraction method for the determination of Rhodamine B in cosmetic products

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dc.contributor.authorDalmaz, Aslıhan
dc.contributor.authorOzak, Sezen Sivrikaya
dc.date.accessioned2023-07-26T11:58:43Z
dc.date.available2023-07-26T11:58:43Z
dc.date.issued2022
dc.departmentDÜ, Sağlık Bilimleri Enstitüsü, Doğal, Bitkisel Ürünler ve Kozmetik Ürünler Ana Bilim Dalıen_US
dc.description.abstractGreen synthesis of clinoptilolite zeolite/Fe3O4 nanocomposite (MZNC) was carried out using Laurus Nobilis L. leaf extract. Characterization of this MZNC was performed using Scanning Electron Microscopy, Fourier Transform Infrared Spectroscopy, X-Ray Diffraction and Vibrating Sample Magnetometer. According to the VSM analysis results, the saturation magnetization of 23 emu/g and coercivity of 23.5 Oe indicate that the synthesized magnetic nanocomposite is superparamagnetic. A new ultrasonic assisted clinoptilolite zeolite-coated magnetic nanocomposite-based solid phase microextraction (MZNC-SPME) method com-bined with high performance liquid chromatography was developed for the extraction and determination of Rhodamine B. The preconcentration factor for the MZNC-SPME method was found to be 40 under opti-mal conditions. Under optimal conditions, the linear range, correlation coefficient (R 2 ), limit of detection (LOD), and intra-and interday relative standard deviation (RSD) were found to be 1.0 0-10 0.0 0 ng mL -1, 0.9995, 0.16 ng mL(-1), 1.89% and 2.49%, respectively. The developed method was successfully performed to determine Rhodamine B in 6 different cosmetic samples. 6 ions and 5 different dyes were added to the sample solution to show the selectivity of the method. The obtained results show that the determination of Rhodamine B is possible in the presence of these ions and dyes. In order to determine the accuracy of the MZNC-SPME method, two different concentrations of Rhodamine B concentration in cosmetic sam-ples were added as 10 and 50 ng mL -1. Extraction recoveries were found in the range of 92.03-101.52% and these results are quite satisfactory. It is seen that the developed method for the extraction and deter-mination of Rhodamine B from cosmetic samples is applicable due to the easy synthesis of the sorbent and the short, simple, environmentally friendly and low cost of the method.(c) 2022 Elsevier B.V. All rights reserved.en_US
dc.description.sponsorshipDuzce University Scientific Research Projects Fund [2022-05-03-1327]; Turkey's Council of Higher Education (CoHE) [10 0/20 0 0]; Duzce University Sci-entific Research Projects Fund; CoHEen_US
dc.description.sponsorshipThis research was supported by Duzce University Scientific Research Projects Fund (Project No: 2022-05-03-1327) and Turkey's Council of Higher Education (CoHE) 10 0/20 0 0 doctoral scholarship program. The authors would like to thank the Duzce University Scientific Research Projects Fund and CoHE for contributing to the financial portion of the project.en_US
dc.identifier.doi10.1016/j.chroma.2022.463433
dc.identifier.issn0021-9673
dc.identifier.issn1873-3778
dc.identifier.pmid36030568en_US
dc.identifier.scopus2-s2.0-85136481672en_US
dc.identifier.scopusqualityQ1en_US
dc.identifier.urihttps://doi.org/10.1016/j.chroma.2022.463433
dc.identifier.urihttps://hdl.handle.net/20.500.12684/13552
dc.identifier.volume1680en_US
dc.identifier.wosWOS:000852681700008en_US
dc.identifier.wosqualityQ2en_US
dc.indekslendigikaynakWeb of Scienceen_US
dc.indekslendigikaynakPubMeden_US
dc.indekslendigikaynakScopusen_US
dc.institutionauthorDalmaz, Aslıhan
dc.institutionauthorSivrikaya Özak, Sezen
dc.language.isoenen_US
dc.publisherElsevieren_US
dc.relation.ispartofJournal of Chromatography Aen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.snmz$2023V1Guncelleme$en_US
dc.subjectRhodamine B; Clinoptilolitezeolite; Fe 3 O 4 Nanocomposite; Laurus Nobilis L; Green Synthesis; Cosmetic Producten_US
dc.subjectCloud-Point Extraction; Waste-Water; Nanoparticles; Preconcentration; Samples; Adsorption; Removal; Liquid; Optimization; Separationen_US
dc.titleDevelopment of clinoptilolite zeolite-coated magnetic nanocomposite-based solid phase microextraction method for the determination of Rhodamine B in cosmetic productsen_US
dc.typeArticleen_US

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