Synthesis and anticorrosion studies of 4-[(2-nitroacetophenonylidene)-amino]-antipyrine on SAE 1012 carbon steel in 15 wt.% HCl solution

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dc.authoridCAKMAK, Resit/0000-0003-0401-7419
dc.authoridKAYA, ERTUGRUL/0000-0003-1579-6411
dc.authoridSolomon, Moses/0000-0002-3251-8846
dc.authoridGerengi, Husnu/0000-0002-9663-4264
dc.authorwosidCAKMAK, Resit/ABA-6424-2020
dc.authorwosidKAYA, ERTUGRUL/AAD-3003-2019
dc.authorwosidSolomon, Moses/I-3762-2016
dc.authorwosidGerengi, Husnu/W-3898-2018
dc.contributor.authorGerengi, Husnu
dc.contributor.authorCakmak, Resit
dc.contributor.authorDag, Besir
dc.contributor.authorSolomon, Moses M.
dc.contributor.authorTuysuz, Hatice Aslihan Akbal
dc.contributor.authorKaya, Ertugrul
dc.date.accessioned2021-12-01T18:49:29Z
dc.date.available2021-12-01T18:49:29Z
dc.date.issued2020
dc.department[Belirlenecek]en_US
dc.description.abstractA novel corrosion inhibitor, ((E)-1,5-dimethyl-4-((1-(3-nitrophenyl)ethylidene)amino)-2-phenyl-1,2-dihydro-3H-pyrazol-3-one) (DNPP) was synthesized in high yield by the condensation reaction of 4-aminoantipyrine with 2-nitroacetphenone derived from acetophenone as a starting material and characterized by FT-IR,H-1, and(13)C NMR techniques. DNPP was tested against the corrosion of SAE 1012 carbon steel in 15 wt.% HCl solution using electrochemical and surface characterization techniques. Results obtained show that DNPP is effective in retarding the corrosion of SAE 1012 carbon steel. With 4 mM of DNPP, the charge transfer resistance of SAE 1012 in 15 wt.% HCl solution is raised from 17.42 to 140.50 ohm cm(2)and the substrate surface is protected by 87%. The inhibition is through adsorption mechanism (mixed-adsorption type) and has been confirmed by SEM and EDAX results. Potentiodynamic polarization results reveal that DNPP acted as a mixed-type corrosion inhibitor. DNPP is a promising candidate for the formulation of an inhibitor cocktail for the strong acid environment.en_US
dc.description.sponsorshipDuzce University Research FundDuzce University [2019.06.05.941]en_US
dc.description.sponsorshipThe present work was financially supported by the Duzce University Research Fund (Project No: 2019.06.05.941).en_US
dc.identifier.doi10.1080/01694243.2020.1766400
dc.identifier.endpage2466en_US
dc.identifier.issn0169-4243
dc.identifier.issn1568-5616
dc.identifier.issue22en_US
dc.identifier.scopus2-s2.0-85086256689en_US
dc.identifier.scopusqualityQ2en_US
dc.identifier.startpage2448en_US
dc.identifier.urihttps://doi.org/10.1080/01694243.2020.1766400
dc.identifier.urihttps://hdl.handle.net/20.500.12684/10729
dc.identifier.volume34en_US
dc.identifier.wosWOS:000541175300001en_US
dc.identifier.wosqualityQ3en_US
dc.indekslendigikaynakWeb of Scienceen_US
dc.indekslendigikaynakScopusen_US
dc.language.isoenen_US
dc.publisherTaylor & Francis Ltden_US
dc.relation.ispartofJournal Of Adhesion Science And Technologyen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.subject4-aminoantipyrineen_US
dc.subjectSchiff baseen_US
dc.subjectCarbon steelen_US
dc.subjectCorrosionen_US
dc.subjectCorrosion inhibitionen_US
dc.subjectCorrosion Inhibition Behavioren_US
dc.subjectMild-Steelen_US
dc.subjectSynergistic Inhibitionen_US
dc.subjectAcidic Mediaen_US
dc.subjectSchiff-Basesen_US
dc.subject2-Mercaptothiazolineen_US
dc.subjectDerivativesen_US
dc.subjectAluminumen_US
dc.subjectChitosanen_US
dc.subjectIodideen_US
dc.titleSynthesis and anticorrosion studies of 4-[(2-nitroacetophenonylidene)-amino]-antipyrine on SAE 1012 carbon steel in 15 wt.% HCl solutionen_US
dc.typeArticleen_US

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