Preparation of poly(AAm-co-HEMA)/ZnO nanocomposites via in situ polymerization/hydrothermal method and determination of their properties

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dc.authoridaksu, mecit/0000-0002-9864-727X
dc.authorwosidaksu, mecit/J-5404-2012
dc.contributor.authorErol, İbrahim
dc.contributor.authorAksu, Mecit
dc.contributor.authorGürler, Zeki
dc.date.accessioned2023-07-26T11:55:30Z
dc.date.available2023-07-26T11:55:30Z
dc.date.issued2022
dc.departmentDÜ, Fen-Edebiyat Fakültesi, Kimya Bölümüen_US
dc.description.abstractIn this study, nanocomposites of acrylamide (AAm) and 2-hydroxyethyl methacrylate (HEMA)-based hydrogel containing ZnO nanoparticles in different ratios by mass (1, 3, and 5%) were synthesized using in situ polymerization/hydrothermal method. It was determined that the hydrogel contained 60% HEMA in the copolymer composition calculated with the help of H-1-NMR. Characterization of materials was carried out by SEM, BET, FTIR, UV-Vis, TGA, and XRD techniques. The Ea and Tg value and thermal stability of the pure poly(AAm-co-HEMA) hydrogel were increased by adding ZnO. The water absorption capacity of nanocomposites was determined by swelling experiments. As the amount of ZnO in the composites increased, the degree of swelling decreased. Biological activities of poly(AAm-co-HEMA) and nanocomposites against gram-positive (S. aureus) and gram-negative (E. coli) bacteria increased as the amount of ZnO increased. Finally, The dielectric properties of the poly(AAm-co-HEMA) and nanocomposites were investigated as a function of frequency at 25 degrees C temperature in the frequency range of 1-200 kHz.en_US
dc.description.sponsorshipAfyon Kocatepe University Scientific Research Projects Coordination Unit [21-FENED-05]en_US
dc.description.sponsorshipThis study has been supported by the Afyon Kocatepe University Scientific Research Projects Coordination Unit. The Project Number is 21-FENED-05.en_US
dc.identifier.doi10.1007/s00289-022-04343-7
dc.identifier.issn0170-0839
dc.identifier.issn1436-2449
dc.identifier.scopus2-s2.0-85133292173en_US
dc.identifier.scopusqualityQ2en_US
dc.identifier.urihttps://doi.org/10.1007/s00289-022-04343-7
dc.identifier.urihttps://hdl.handle.net/20.500.12684/13085
dc.identifier.wosWOS:000819702900001en_US
dc.identifier.wosqualityQ2en_US
dc.indekslendigikaynakWeb of Scienceen_US
dc.indekslendigikaynakScopusen_US
dc.institutionauthorAksu, Mecit
dc.language.isoenen_US
dc.publisherSpringeren_US
dc.relation.ispartofPolymer Bulletinen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.snmz$2023V1Guncelleme$en_US
dc.subjectPoly(Aam-Co-Hema) Hydrogels; In Situ Polymerization; Hydrothermal Method; Thermal Stability; Antibacterial Activity; Swellingen_US
dc.subjectZno Nanoparticles; Biological Evaluation; Acrylamide Derivatives; Dielectric-Properties; Metabolic Stability; Hydrothermal Method; Zinc-Oxide; Thin-Films; Methacrylate; Photoluminescenceen_US
dc.titlePreparation of poly(AAm-co-HEMA)/ZnO nanocomposites via in situ polymerization/hydrothermal method and determination of their propertiesen_US
dc.typeArticleen_US

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