A novel vortex-assisted liquid phase microextraction method for parabens in cosmetic oil products using deep eutectic solvent

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dc.contributor.authorSivrikaya, Sezen
dc.date.accessioned2020-04-30T22:38:48Z
dc.date.available2020-04-30T22:38:48Z
dc.date.issued2019
dc.departmentDÜ, Teknoloji Fakültesi, Polimer Mühendisliği Bölümüen_US
dc.descriptionWOS: 000471435400001en_US
dc.description.abstractThe parabens, which are harmful to our bodies, are primarily utilized as preservatives in medicine, personal care products and cosmetics. A novel, more efficient, fast and cheap vortex-assisted liquid phase microextraction method based on deep eutectic solvents (DESs) was developed for the determination of parabens. The microextraction conditions were optimized using these solvents and the analytical parameters of the method were determined under optimal microextraction conditions. After extraction, the chromatographic separation of parabens was undertaken using high-performance liquid chromatography-UV detection. Experimental parameters, such as DES type, DES volume, dilution solvent volume and vortex extraction time were optimized. DES6 [ChCl-Ethylene glycol (1/2)] was the most suitable DES to work in this study. Detection limits for this method of 0.053 mu g mL(-1) for methylparaben, 0.061 mu g mL(-1) for ethylparaben, 0.049 mu g mL(-1) for propylparaben and 0.052 mu g mL(-1) for butylparaben were obtained. Correlation coefficients (R-2) for a concentration range of 0.1-100 mu g mL(-1) were higher than 0.9992 and relative standard deviation (RSD) values below 2.91% at parabens concentration of 2.5 mu g mL(-1) were obtained. The results of spike/recovery values of real samples were greater than 84%. When compared with other methods, the main advantages include lower LOD, short extraction time, rapidity, repeatability and simplicity.en_US
dc.description.sponsorshipDuzce University Research Project FoundationDuzce University [2018.07.06.803]en_US
dc.description.sponsorshipThis work was supported by a grant from Duzce University Research Project Foundation (Project no: 2018.07.06.803).en_US
dc.identifier.doi10.1080/03067319.2019.1625345en_US
dc.identifier.endpage1585en_US
dc.identifier.issn0306-7319
dc.identifier.issn1029-0397
dc.identifier.issue15en_US
dc.identifier.scopusqualityQ3en_US
dc.identifier.startpage1575en_US
dc.identifier.urihttps://doi.org/10.1080/03067319.2019.1625345
dc.identifier.urihttps://hdl.handle.net/20.500.12684/2452
dc.identifier.volume99en_US
dc.identifier.wosWOS:000471435400001en_US
dc.identifier.wosqualityQ4en_US
dc.indekslendigikaynakWeb of Scienceen_US
dc.indekslendigikaynakScopusen_US
dc.language.isoenen_US
dc.publisherTaylor & Francis Ltden_US
dc.relation.ispartofInternational Journal Of Environmental Analytical Chemistryen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.subjectParabensen_US
dc.subjectdeep eutectic solventsen_US
dc.subjectvortex-assisted liquid phase microextractionen_US
dc.subjectcosmetic oilsen_US
dc.titleA novel vortex-assisted liquid phase microextraction method for parabens in cosmetic oil products using deep eutectic solventen_US
dc.typeArticleen_US

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