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Öğe Comparison between NiO and MnO2 nanoparticles deposited on graphene-coated nickel foam for water purification applications(Elsevier, 2023) AlAnazi, Maha; Ghrib, Taher; Ercan, Filiz; Kotb, Essam; Bubshait, Ruqaiyah; Almilad, Fatimah; Elibol, ErdemNanoparticles of NiO, and MnO2 nanoparticles were successfully synthesized on graphene-coated Nickel foam (NFG) substrates for the synthesis of dual-functional specimens for antibacterial and photocatalytic applications. The morphological, structural, and optical properties were investigated thanks to the techniques of scanning electron microscopy (SEM), Fourier-transform infrared spectroscopy (FTIR), X-ray diffraction (XRD), UV-Vis, and photoluminescence spectroscopy. It was observed from XRD analysis that alpha-MnO2 and NiO nanoparticles were deposited with high purity as a thin film on NFG substrates. The photocatalytic efficiency of the synthesized materials was tested on a Methylene blue (MB) solution as a target dye pollutant and the obtained results indicate a good degradation rate under visible light irradiation. Antibacterial activity was tested on Staph aureus, Pseudomonas aeruginosa, and the yeast Candida albicans. The obtained results show that MnO2/NFG and NiO/NFG specimens constitute good candidates for the treatment of wastewater.Öğe Effect of Al0.1Ga0.9As thickness on the structural, optical, thermal, and electrical properties of (Al0.1 Ga 0.9As)/GaAs heterojunctions(Elsevier Ltd, 2023) Al-Naghmaish, Aishah; Ghrib, Taher; Dakhlaoui, H.; AL-Saleem, N.K.; Ercan, F.; Kayed, Tarek S.; Elibol, ErdemAl0.1Ga0.9As nano-films of various thicknesses were deposited on GaAs substrate and examined using Scanning Electron Microscopy (SEM), X-Ray Diffraction (XRD), UV–Visible spectrophotometry, Photoluminescence (PL), Electrochemical Impedance Spectroscopy (EIS), and Photothermal Deflection (PTD). The PTD technique is used to analyze the effect of Al0.1Ga0.9As thickness on thermal properties and showed its sensitivity to weak structural changes. By increasing the Al0.1Ga0.9As thickness, the crystallinity was degraded, an infrared emission centered at 997.4 nm whose intensity is the highest for 50 nm was observed. A pn junction was formed for thicknesses higher than 400 nm, the band gap was increased from 1.59 to 1.68 eV. The thermal conductivity increased from 35.3 to 37.3 W m? 1 K?1 and the thermal diffusivity increased from 0.195 to 0.22 cm2 s?1. As a result of this investigation, the Al0.1Ga0.9As/GaAs can be considered for potential applications in photoelectric and thermoelectric devices. © 2023 The Author(s)Öğe Structural, magnetic and gamma-ray shielding features of cerium doped Mg2FeTiO6 double perovskite(Elsevier, 2023) Saleh, Noha A.; Alqahtani, Muna Y.; Mhareb, M. H. A.; Ercan, Filiz; Ghrib, Taher; Kayed, Tarek S.; Özçelik, BekirThe Mg2FeTi1-xCexO6 [ x = (0, 2, 4, 6, 8, 10)%] ceramics with different Ce concentrations have been pre-pared by solid-state technique. That compounds were doped with cerium dioxide (CeO2) to develop new material for gamma radiation shielding. The prepared nanomaterials were analyzed to investigate their structural and optical properties by XRD, FTIR, SEM, magnetic properties, and UV techniques. It was de-termined by the XRPD method that the atomic and molecular structures of Ce-doped compounds were in the tetragonal crystal system and crystallized in the P4/mmm (No: 123) space group. The refinement parameters of the compound Ce doped x = 8% were gof 2.4 and Rf 0.82. The effect of the Ce doping on the magnetization was measured in the magnetic field ranging at +/- 10 kOe for two temperatures (300 and 10 K) and showed that its Saturation Magnetization (Ms) was increased with the doping increase from 6.2 to 8.1 and from 14.7 to 18.7 for the temperatures 300 and 10 K, respectively. Various radiation shielding parameters for gamma-rays, neutron, and proton were evaluated using Phy-X and SRIM soft -wares. The linear attenuation coefficient (LAC) increases gradually with adding CeO2 to Mg2FeTiO6 from 54.290 to 92.032 cm -1 at 0.015 MeV. Also, fast neutron removal cross-section ( ER ) rises from 0.077 to 0.115 cm-1 for x = 0 and x = 10%. While the sample x = 10% shows the lowest projectile range for pro-tons. This sample considers the best sample to stop protons. The Analysis demonstrates that the sample with x = 10% shows the highest gamma, proton, and neutron shielding properties nominated it to use in radiation shielding field.(c) 2022 Elsevier B.V. All rights reserved.Öğe Structural, optical and photocatalytic properties of cerium doped Ba2TiMoO6 double perovskite(Elsevier B.V., 2023) Ghrib, Taher; Al-Otaibi, A.; Ercan, F.; Manda, Abdullah A.; Özçelik, Beraat; Ercan, İsmailCe doped Ba2TiMoO6 nanomaterials with different Ce concentrations were synthesized by solid state technique. It was determined by the XRPD method that the atomic and molecular structures of Ba2Ti1-xCexMoO6 [x=(1,3,5,7)%] compound was in the tetragonal crystal system and crystallized in the P4mm space group. The purification parameters were found to be gof 1.2 and Rf 1.60. The Scanning Electron Microscopy, Transmission Electron Microscopy, and surface area analysis were used to examine the surface morphology. The UV–Vis diffuse reflectance and photoluminescence spectroscopies were used to investigate the optical properties. The study results showed the successful synthesis of pure and Ce doped Ba2TiMoO6 nanopowders, characterized by 8–20 nm grain size, 3.41–3.6 eV bandgap, and violet emission at 426.67 nm wavelength. The photocatalytic activities of the produced samples were tested against Methyl and it was observed that these activity values increased with the percentage of Ce doping. © 2022 Elsevier B.V.Öğe Structural, optical, and electrical investigation of multilayered MnO2(n)/ NiO(p) heterojunctions for supercapacitors applications(Elsevier, 2023) Alanazi, Maha; Ghrib, Taher; Ercan, Filiz; Alsubaie, Mizna; Demirci, Tuna; Kaygili, Omer; Kayed, Tarek S.Heterojunctions of alternating MnO2 and NiO thin films were deposited on an Indium Tin Oxide (ITO). The MnO2 and NiO thin films were synthesized by electrodeposition and sol-gel methods respectively. The structural morphology of the synthesized heterojunctions was investigated by scanning electron microscopy (SEM) and atomic force microscopy (AFM). The microstructural and chemical compositions were examined by X-ray diffraction (XRD), Fourier transform infrared (FTIR), and Raman techniques. The optical properties were investigated by Ultraviolet-Visible (UV) analysis. The electrical conductivity, specific capacitance, and charge carrier density were determined using the Hall effect and Electrochemical impedance spectroscopy (EIS) methods. As a result, it was found that the MnO2 and NiO thin films crystallize in tetragonal and cubic crystal systems respectively. Increasing the number of NiO/MnO2 heterojunctions increases the electrical conductivity from 9.7 x 10- 7 to 1.2 x 10-3 S.cm- 1, the bandgap decreased 3.16 to 2.62 eV, the volume carrier density rises from 5.17 x 1011 to 4.62 x 1012 cm-3. The specimens constituted of two and four alternative staked MnO2 and NiO layers are characterized by a specific capacitance of 3.6 x 103 and 5.8 x 103 F.g -1 and capacitance retention of 14.8 and 12.9% which consider them promising materials for supercapacitor devices.Öğe Structural, optical, and electrical properties of Zn(1-x)MgxO nano-compounds and ZnO/Zn(1-x)MgxO heterostructures(Elsevier Science Sa, 2022) Ercan, Filiz; Alamroo, Nabilah; Ghrib, Taher; Kayed, Tarek; Özçelik, Bekir; Ercan, İsmail; Alonizan, NorahIn this study, the structural, thermal, optical, electrical and magnetic properties of Zn(1-x)MgxO (x = 0.0, 0.1, 0.3, 0.5) nano-compounds obtained by the addition of MgO to pure ZnO nano-compounds obtained by solid state reaction were investigated in detail. These nanomaterials were deposited by spin coating technique in hetero-structure of ZnO/Zn(1-x)MgxO. It was found by detailed structure solution that the crystal systems of nano materials obtained with MgO additive remained hexagonal, but the space group was transferred from P63mc to P6/mmm. The thermal gravimetry analysis shows the stability of prepared nanomaterials, the UV-Vis spectroscopy shows that the bandgap of the prepared was decreased from 3.02 to 2.52 eV with the Mg doping percentage. The Magnetization measurements at room temperature showed that all four of these Zn(1-x)MgxO nanostructures exhibited soft ferromagnetic behavior. The analysis of the ZnO/Zn(1-x)MgxO heterostructure showed that its band gap was increased from 3.69 to 3.79 eV, its carrier density was decreased from 1.14 x 10(19) to 4.20 x 10(13 )cm(-3) which introduce it as a good material to be used in optoelectronic devices field.Öğe Structural, Optical, Dielectric and Magnetic Properties of Double Perovskite Oxides A(2)FeTiO(6) (A = Zn, Mg, Cu) Nanopowders(Springer Heidelberg, 2022) Ghrib, Taher; Ercan, Filiz; Kayed, T. S.; Flemban, Tahani H.; Yıldız, Mesut; Kaygılı, Ömer; Ercan, İsmailThe investigation of structural, microstructural, optical, dielectric, and magnetic properties of double perovskite materials Zn2FeTiO6 (M1), Mg2FeTiO6 (M2), and Cu2FeTiO6 (M3) synthesized by solid-state reaction was reported in this work. The three compounds crystalized in a monoclinic structure with the space group of P12(1)/c. The microstructure of M1, M2, M3 samples was scanned by SEM to show the crystallinity in shape, and elemental mappings from EDX confirmed the consistency with sample concentrations. Similar spectra were observed from the FTIR technique. The diffused reflectance in the 200-800 nm wavelength range and photoluminescence for the samples were measured to investigate the optical properties. Dielectric constants, conductivity, frequency dependence of the tangent loss (tan delta), AC conductivity at different dc bias voltages, and the electric modulus M(omega) were examined to ensure the potential of the examined materials for microelectronic applications in circuit devices.
