Aksu, Mecit2020-04-302020-04-3020140970-7077https://dx.doi.org/10.14233/ajchem.2014.18221https://hdl.handle.net/20.500.12684/335In this work V2O5 was reduced to sodium intercalated NaV2O5 with NaBH4 in pyridine-water solvent. Techniques to investigate the composition, crystallinity and morphology of products as prepared include field emission scanning electron microscopy, energy dispersive X-ray spectroscopy and X-ray powder diffraction inductively coupled plasma-atomic emission spectroscopy. Unit cell parameters are a = 11.28, b = 3.583, c = 4.76 Å and ? = ?b = ? = 90° . Mean crystallite size was calculated to be 4.8 nm.en10.14233/ajchem.2014.18221info:eu-repo/semantics/openAccessNaBH4; Nano (na)v2 o5; V2o5.Article262382598260Q4